General stuff:
Letter
Teams
Syntheses for teams (OS recipes can be found at http://www.orgsyn.org/)
Recepies
Program
About synthesis - By Mikael Begtrup
Submission after each synthesis
Exam assignment
Evaluation form
Lecture notes:
Introduction (Pittelkow)
About organic synthesis (Begtrup)
Chromatography (Tortzen). DCVC guide. Original flash paper. DCVD paper.
Process chemistry (Haakansson/Lundbeck)
Electrochemistry (Hammerich).
Flow chemistry and microwave synthesis (Glasnov/Graz)
Smelly compounds (Stuhr-Hansen)
Metal-organic chemistry (Parker)
Choice of bases (Begtrup)
Solid-phase chemistry (Jensen)
Fairy tales (Begtrup)
Techniques (Brock-Nannestad)
Videos illustrating techniques (large files, so it might be slow):
- The plastic bag technique (titration of t-BuLi).
- The double septa technique to handle reactive liquids (titration of t-BuLi).
- In situ generation of CO using a two chamber technique.
- Synthesis of resin bound PPh3.
- Fun with photo-switch! | 