General stuff:
Letter
Teams
Syntheses for teams (OS recipes can be found at http://www.orgsyn.org/)
Recepies
Program
About synthesis - By Mikael Begtrup
Submission after each synthesis
Exam assignment
Evaluation form
Lecture notes:
Introduction (Pittelkow/KU)
About organic synthesis (Begtrup/KU)
Chromatography (Tortzen/KU). DCVC guide. Original flash paper. DCVD paper.
Metal-organic chemistry (Parker/Syntese)
Electrochemistry (Hammerich/KU)
Flow chemistry (Lindhardt/Aarhus)
Process chemistry (Kehler/Lundbeck)
Choice of bases (Begtrup/KU)
Fairy tales (Christensen/KU)
Fairy tales (Begtrup/KU)
High energy materials (Peterson/Cambridge UK)
Videos illustrating techniques (large files, so it might be slow):
- The plastic bag technique (titration of t-BuLi).
- The double septa technique to handle reactive liquids (titration of t-BuLi).
- In situ generation of CO using a two chamber technique.
- Synthesis of resin bound PPh3.
- Fun with photo-switch! |